Determination of fumonisins in edible vegetable oil by MIL-101(Cr) based dispersive solid-phase extraction combined with high-performance liquid chromatography-tandem mass spectrometry
文献类型： 外文期刊
作者： Yang, Ming 1 ; Yi, Jun 1 ; Wei, Cong 3 ; Peng, Xitian 4 ; Yang, Zong 5 ; Zhao, Liuqin 5 ; Jiang, Xiaoming 1 ; Tu, Fengqin 1 ;
作者机构： 1.Wuhan Inst Food & Cosmet Control, Wuhan 430040, Peoples R China
2.Key Lab Natl Market Supervis Edible Oil Qual & Saf, Wuhan 430040, Peoples R China
3.Sixth Hosp Wuhan, Wuhan 430015, Peoples R China
4.Hubei Acad Agr Sci, Inst Agr Qual Stand & Testing Technol Res, Hubei Key Lab Nutr Qual & Safety Agro Prod, Wuhan 430064, Peoples R China
5.Aisa Pacific Tech Support Ctr SCIEX, Shanghai 200050, Peoples R China
关键词： Fumonisins; MIL-101 (Cr); Dispersive solid-phase extraction; HPLC-MS; MS; Edible vegetable oil
期刊名称：JOURNAL OF FOOD COMPOSITION AND ANALYSIS （ 影响因子：4.3； 五年影响因子：4.6 ）
ISSN： 0889-1575
年卷期： 2023 年 117 卷
页码：
收录情况： SCI
摘要： A method was first developed based on MIL-101(Cr) dispersive solid-phase extraction for determining fumonisins in edible vegetable oil. Fumonisins contain hydroxyl and carboxyl groups and were easily adsorbed by MIL-101 (Cr) with intermolecular force. With the matrix matching the external standard method for quantification, several extraction factors such as extraction solvent, adsorption dose, extraction time, desorption solvent, desorption solvent volume, desorption time, and filter membrane were optimized. The linear ranges were 5.0-40 mu g/L, and the correlation coefficients (r) were greater than 0.9997. The LODs and LOQs of the target analyte were 1.5 and 5.0 mu g/kg. At the four spiked concentrations (5, 10, 20, and 40 mu g/kg), the recovery rates were between 94.5% and 101.7%, and the RSDs were between 2.02% and 5.32%. The inter-day and intra-day tests recoveries were 98.5%- 99.9% and 93.7%- 98.7%, respectively. The precision of the inter-day and intra-day analysis was 5.09-6.05% and 2.56%- 3.19%, respectively. The pretreatment time of this method is only 1 h, and the efficiency is 4-8 times higher than that of other methods.These results showed that the method was fast, selective, low cost, and sensitive and had obvious advantages for accurately determining and analyzing fumonisins in edible oil samples.
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